Quantitative Headspace Solid-Phase Microextraction Gas Chromatography Mass Spectrometry (HS-SPME-GC-MS/ MS) Method for the Determination of Tributyltin in Sediment: Validation according to EU Directive Requirement
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منابع مشابه
Identification of Honey Volatile Components by Solid Phase Microextraction (spme) and Gas Chromatography/mass Spectrometry (gc/ms)
Volatile compounds in honey samples of different botanical origins were investigated. Solid phase microextraction (SPME) and gas chromatography-mass spectrometry (GC/MS) revealed a total of 86 compounds in the headspace of 4 types of honey – multifloral, heather, buckwheat and lime-honeydew. The chemical composition of the headspace was very diverse, owing to the presence of compounds from diff...
متن کاملAnalysis of the volatile components of five Turkish Rhododendron species by headspace solid-phase microextraction and GC-MS (HS-SPME-GC-MS).
Volatile constituents of various solvent extracts (n-hexane, CH2Cl2, H2O) of 15 different organs (leaves, flowers, fruits) of five Rhododendron species (Ericaceae) growing in Turkey were trapped with headspace solid-phase microextraction (HS-SPME) technique and analyzed by GC-MS. A total of 200 compounds were detected and identified from organic extracts, while the water extracts contained only...
متن کاملDetermination of volatile aroma compounds of Ganoderma lucidum by gas chromatography mass spectrometry (HS-GC/MS).
This study was conducted at Horticulture Department of Cukurova University, Adana, Turkey during 2010-2011. Fresh sample of Ganoderma lucidum collected from Mersin province of Turkey was used as material. Volatile aroma compounds were performed by Headspace Gas Chromatography (HS-GC/MS). Alcohols, aldehydes, acids, phenol, L-Alanine, d-Alanine, 3Methyl, 2-Butanamine, 2-Propanamine were determin...
متن کاملDetermination of oxadiazon residues by headspace solid-phase microextraction and gas chromatography-mass spectrometry.
A method for the determination of trace amounts of the herbicide oxadiazon was developed using headspace solid-phase microextraction (HS-SPME), gas chromatography-mass spectrometry (GC-MS) and selected ion monitoring. It was applied to determine oxadiazon in ground water, agricultural soil, must, wine and human urine samples. To determine oxadiazon in liquid samples, a response surface methodol...
متن کاملApplications of solid-phase microextraction and gas chromatography/mass spectrometry (SPME-GC/MS) in the study of grape and wine volatile compounds.
Volatile compounds are responsible for the wine "bouquet", which is perceived by sniffing the headspace of a glass, and of the aroma component (palate-aroma) of the overall flavor, which is perceived on drinking. Grape aroma compounds are transferred to the wine and undergo minimal alteration during fermentation (e.g., monoterpenes and methoxypyrazines); others are precursors of aroma compounds...
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ژورنال
عنوان ژورنال: SM Analytical and Bioanalytical Techniques
سال: 2017
ISSN: 2573-3729
DOI: 10.36876/smabt.1007